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Revisiting the Hinsberg reaction: Facile and expeditious synthesis of 3-substituted quinoxalin-2(1H)-ones under catalyst-free conditions in water
Substituted benzene-1,2-diamine reacted with various alpha-keto esters at 50 under mild conditions for 15 min using H2O as reaction medium, providing a variety of 3-substituted quinoxalinone derivatives in excellent yields. The reaction was instantaneous, and products were isolated by simple filtration.
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Chiral Catalysts,
Chiral catalysts – SlideShare